INSTITUTO POLITÉCNICO NACIONAL
ESCUELA SUPERIOR DE INGENIERÍA QUÍMICA E INDUSTRIAS EXTRACTIVAS LABORATORIO DE TÉCNICAS DE POLIMERIZACIÓN Y FORMULACIÓN DE LOS POLÍMEROS
PRÁCTICA No.4 “FORMULACIÓN DE UN PLASTISOL” PROFESOR: RICARDO SANTILLÁN P. GRUPO:
DIAGRAMA DE BLOQUES Practica 4 F!"#$%&'()* +, $* -%&/(!%”
EQUIPO: 1
Material: • • • • •
Resina PVC DOP DBP CaCO 3 NaHCO3
Paso : Pesar en un !aso la resina de PVC
Paso 4: '&re&ar el DOP y DBP a la ecla* a&itar constanteente#
Paso $: una !e teniendo una ecla uni+ore se coloca en el olde con la +ora deseada y se ete al .orno a %01C
Paso 2: Pesar el DOP y el DBP (liquidos) en otros
Paso 3: Pesar el CaCO 3 y el NaHCO3* eclando con la resina de PVC
Paso ,: Re!isar cuidadosaente cada $ in !iendo que el -lastisol .aya solidi/cado
Paso : Dear en+riar y des-us desoldar -ara o5tener el -lastisol con la
TABLA DE CANTIDADES AGREGADAS
SUSTANCIA
EQUIPO 1
EQUIPO 2
EQUIPO 3
EQUIPO 4
EQUIPO 5
EQUIPO 6
RESINA PVC
10.2345
10.2345
10.2345
10.2345
16.76615
89
DOP
19.49725
95
7.46195
8.0225
19.49725
75
DBP
95
19.49725
8.0225
7.46195
95
95
CaC O 3
9.07665
9.07665
9.07665
9.07665
.28035
95
NaHC O3
.46195
.46195
.46195
.46195
.28035
35
ANÁ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
OBSERVACIONES Y CONCLUSIONES ,% ",&%(&" -%&/(!% *! , $*& '(,*'(& #$; '!#-%('&+& #& (* ,#=&"5! &; ?$, '!*!'," %& $*'(!*&=(%(+&+ +, '&+& $*! +, %! ,%,#,*/! ?$, '!*/(,*, -&"& -!+," ",&%(&" $*& #,!"& +,*/"! +, %& #(#&. E* '$&*/! ,% ,-$#&*/, ,% ",$%/&+! *! $, ,% ,-,"&+! ;& ?$, ,% '",'(#(,*/! +, %& -(,& $, -"'/('&#,*/, (#-,"',-/(=%,. L& '&"5& ",&%(&* $ /"&=&! +, &=&"&/&#(,*/! -,"! *! %, &-!"/&* $*& 5"&* ",(/,*'(& -!" %! ?$, -$,+! ,-,'$%&" ?$, ,/$@! ,* -"!-!"'()* =&& ! '&#=(&"%& -!" &%5* !/"& ?$, %, !/!"5$, $* -!'! #& +, ,%&/('(+&+ -,"! +$",& -&"& +(#(*$(" %& '$&"/,&+$"& !=,"@&+& ,* /!+& %& -(,&.
CUESTIONARIO Expl!"# #l #$#%&o !"# &#'# #l (%)#*+ %,*-, pl,/&$%,'&#/ #' l, #/&*"%&"*, 0# l, %#l0, 0# pl,/&/ol#/ #/p"1,0o. E% &5,*/, ,-$#&*/, /(,*, ,% ,,'/! +, ,-&*+(" ,% -"!+$'/! (*&% &% %(=,"&" CO 8 '$&*+! , ,% -"!+$'/! & /,#-,"&/$"& &%/& -&"& ,% '$"&+! L& '&"5& /(,*, %& $*'()* +, +&" +$",& &% -"!+$'/! /,"#(*&+! +, PVC ; /&#=(H* -&"& &=&"&/&" ,% -"!',! +, -"!+$''()* L! -%&/(('&*/, /(,*,* %& $*'()* +, ="(*+&" $*& '(,"/! 5"&+! +, %,(=(%(+&+ (*'",#,*/&*+! %& +(/&*'(& ,*/", %& '&+,*& +,% -!%#,"!
Co1o /# 1o0$%, l, 2/%o/0,0 #' "' pl,/&/ol p,*, '1#*/3' L& @('!(+&+ +, $* P%&/(!% !=/,*(+! -!" ,% -"!',! +, (*#,"()* , #!+(('& +,-,*+(,*+! +,% /(-! +, -%&/(('&*/, &( '!#! /&#=(H* %& '&*/(+&+ +,% #(#!.
Q"# ,0&2o/ 1o0$%,*, p,*, '%*#1#'&,* #l -*,0o 0# #xp,'/3'. E* ,% '&! +,% P%&/(!% ,% &+(/(@! ?$, (*'",#,*/& %& ,-&*()* , ,% ,-$#&*/, JN&KCO ;& ?$, %(=,"& 5&, ?$, , ?$,+&* ,*',""&+! ,* %& ',%+& -!%(#H"('& ; !'$-&* $* @!%$#,* ; ,/! !'&(!*& %& ,-&*()*.
Po* !"5 'o #/ po/6l# o6&#'#* pl,/&/ol#/ %o' *#/',/ 0# PVC #' /"/p#'/3' 7'%,1#'&#
L! -!%#,"! !=/,*(+! #,+(&*/, %& /H'*('& +, $-,*()* ",?$(,",* +, $* #,+(! '!*/(*$!J&5$& ,* +!*+, , ",&%(& %& -!%(#,"(&'()* %! -%&/(!%, , !=/(,*,* ,* $* #,+(! ,* +!*+, ,(/, -%&/(('&*/, ; %! +(,",*/, &+(/(@! &+,# %& ",&''()* -&"& !=/,*," ,% P%&/(!% , +, '!*+,*&'(!*
Q"# 0$#*#'%, #x/&# #' l, %o'%#'&*,%3' P8R #l po*%#'&o p#/o 9. L& '!*',*/"&'()* -" , ",(,", & %& -&"/, -!" '&+& 199 +, -!%#,"! %& -&"/, +, '&+& '!#-$,/! ,* %& !"#$%&'()* +,-,*+,* +, %& '&*/(+&+ +, -!%#,"! ; ,% -,! +,-,*+, +, %& '&*/(+&+ +, !%(+! /!/&, ,* %& !"#$%&'(!*
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
CUESTIONARIO :. Expl!"# #l #$#%&o !"# &#'# #l (%)#*+ %,*-, pl,/&$%,'&#/ #' l, #/&*"%&"*, 0# l, %#l0, 0# pl,/&/ol#/ #/p"1,0o. L& '&"5& /(,*, %& $*'()* +, +&" +$",& &% -"!+$'/! /,"#(*&+! +, PVC ; /&#=(H* -&"& &=&"&/&" ,% -"!',! +, -"!+$''()* L! -%&/(('&*/, /(,*,* %& $*'()* +, ="(*+&" $* '(,"/! 5"&+! +, %,(=(%(+&+ (*'",#,*/&*+! %& +(/&*'(& ,*/", %& '&+,*& +,% -!%#,"!
;.
.
4.
OBSERVACIONES @
L& '&*/(+&+ +, -%&/(!% &5",5&+& &% -"(*'(-(! *! $, $('(,*/, *! -!+&#! #,'%&" =(,* -!" %! '$&% /$@(#! ?$, &5",5&" ,* *$,/"! '&! %! +!=%, +, DOP. L& @,%!'(+&+ +, #,'%&+! (*%$;, #$'! ;& ?$, & #&;!" @,%!'(+&+ #&;!" @('!& , @$,%@, *$,/"& #,'%& , # +('(% ?$, , (*/,5",* /!+!.
CONCLUSIONES F!"#$%&#! $* -%&/(!% '!* ",(*& +, PVC '&+& ,?$(-! !'$-! '&*/(+&+, +(,",*/, ,* #( ,?$(-! *! , $/(%() -%&/(('&*/, DBP< -$+(#! '!#-"!=&" ?$, $*'()* /(,*, '&+& $*! +, %! '!#-!*,*/, -!" ,,#-%! *$,/"& '&"5& CaCO , ,*'&"5) +, #!+(('&" %& -"!-(,+&+, #,'*('& +, *$,/"! -%&/(!% #!+((') 3
%& +$",&. E% NaHC O &'/$) '!#! &5,*/, ,-$#&*/, &$*?$, $, $*& '&*/(+&+ #$; -,?$,& %& ?$, &5",5&#! ; *! ,-$#) %! $('(,*/,. L! '!/! +,-,*+,* #$'! +,% &5,*/, ,-$#&*/, ;& ?$, , ,% ?$, %! @& & ",+$'(" (5*(('&/(@&#,*/,. 3
P!" %/(#! -,"! *! #,*! (#-!"/&*/, ,% -(5#,*/! %, +& $*& @(/& &5"&+&=%, & *$,/"! -%&/(!%.
CUESTIONARIO :. Expl!"# #l #$#%&o !"# &#'# #l (%)#*+ %,*-, pl,/&$%,'&#/ #' l, #/&*"%&"*, 0# l, %#l0, 0# #llo/ pl,/&/ol#/ #/p"1,0o. R L! %%&#&+! ('," ",+$',* %& /,#-,"&/$"& +, +,'!#-!('()* %! ('," /&#=(H* /(,*,* $* ,,'/! ,/&=(%(&+!". ;.
>.
CONCLUSIONES E% -%&/(!% , '!*(+,"&+! $*& #,'%& +, $*& ",(*& $* -%&/(('&*/, ; &%5$*! &+(/(@!. E $* %?$(+! =%&*?$,'(*! '!* -"!-(,+&+, ,%/('&. A% ," '&%,*/&+! -&& +,% ,/&+! %?$(+! &% )%(+! (* -,"+," *(*5$*& +, $ -"!-(,+&+,. A$#,*/& $ @('!(+&+ '$&*+! &$#,*/& %& /,#-,"&/$"& &=&*+!*&*+! $ ,/&+! %?$(+! (*('(&% -&"& %%,5&" &% ,/&+! )%(+!. R,(/, & %& ,%,'/"('(+&+ , +,'(" *! ,
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
BIBLIOGRAFA
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