1. Pengukuran Butiran Padatan

LAPORAN RESMI PRAKTIKUM OPERASI TEKNIK KIMIA I

“PENGUKURAN BUTIRAN PADATAN”

GRUP E

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LABORATORIUM RISET DAN OPERASI TEKNIK KIMIA PROGRAM STUDI TEKNIK KIMIA -AKULTAS TEKNIK UPN “ETERAN” AA TIMUR SURABAA 201/

LAPORAN PRAKTIKUM OPERASI TEKNIK KIMIA I FLUIDISASI UPN “VETERAN” “ VETERAN” JAWA JAWA TIMUR

LEMBAR PENGESA4AN

LAPORAN TUGAS PRAKTIKUM OPERASI TEKNIK KIMIA I

“PENGUKURAN “PENGUKU RAN BUTIRAN PADAT ADATAN”

Telah diperi!a da" di!e#$%$i &leh '

Kepala La(&ra#&ri$) Opera!i Te"i Te"i Ki)ia I

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Program Studi Studi S-1 Teknik Teknik Kimia Fakultas Teknik-UPN Teknik-UPN “VETERAN”JAT! “VETERAN”JAT!

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LEMBAR PENGESA4AN

LAPORAN TUGAS PRAKTIKUM OPERASI TEKNIK KIMIA I

“PENGUKURAN “PENGUKU RAN BUTIRAN PADAT ADATAN”

Telah diperi!a da" di!e#$%$i &leh '

Kepala La(&ra#&ri$) Opera!i Te"i Te"i Ki)ia I

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i


KATA KATA PENGAN PE NGANT TAR

P$%i !7$$r a)i pa"%a#a" epada T$ha" 7a"5 Maha E!a, a#a! (era# da" rah)a#8N7a, !ehi"55a a)i dapa# )e"7ele!aia" Lap&ra" Re!)i Opera!i Te"i Ki)ia I i"i de"5a" %$d$l “Fl$idi!a!i”* Lap&ra Lap&ra" " Re!)i Re!)i i"i )er$pa )er$paa" a" !alah !alah !a#$ #$5a! #$5a! )a#a )a#a $liah $liah pra#i pra#i$) $) Opera!i Opera!i Te"i Ki)ia I 7a"5 di(eria" di(eria" pada !e)e!#er IV* IV* Lap&ra" Lap&ra" i"i di!$!$" (erda!ara" pe"5a)a#a" hi"55a perhi#$"5a" da" dile"5api de"5a" #e&ri dari li#era#$r !er#a pe#$"%$ a!i!#e" pe)(i)(i"5 7a"5 dila!a"aa" pada #a"55al 4Fe(r$ari 41-3 di La(&ra#&ri$) Opera!i Te"i Ki)ia* Lap&ra" ha!il pra#i$) i"i #ida dapa# #er!$!$" !ede)iia" r$pa #a"pa (a"#$a" (ai !ara"a, pra!ara"a, pe)iira", ri#i da" !ara"* !ar a"* Oleh are"a i#$, #ida l$pa a)i $9apa" #eri)a a!ih epada , -* I($ Ir* Ir* +* P$%ia!#$#i,MT !ela$ Kepala La(&ra#&ri$) Opera!i Opera!i Te"i Te"i Ki)ia da" I($ Ir* I!"i U#a)i, MT* 4* Sel$r$h Sel$r$h a!i!#e" d&!e" 7a"5 7a"5 )e)(a"#$ )e)(a"#$ dala) pela!a"aa" pela!a"aa" pra#i$) pra#i$) 0* Rea Rea" " : rea rea" " )aha )aha!i !i!;a !;a 7a"5 7a"5 )e)( )e)(a" a"#$ #$ dala) dala) )e)( )e)(er eri ia" a" )a!$ )a!$a a"8 "8 )a!$a" dala) pra#i$)* Ka)i Ka)i !a"5a# !a"5a# )e"7ad )e"7adari ari dala) dala) pe"7$! pe"7$!$"a $"a" " lap&ra lap&ra" " i"i )a!ih )a!ih (a"7a (a"7a e$ra e$ra"5a "5a"* "* Maa Maa de"5a" de"5a" re"dah re"dah ha#i, ha#i, a)i a)i !elal$ !elal$ )e"5ha )e"5harap rapa" a" ri#i ri#i da" !ara", !el$r$h a!i!#e" d&!e" 7a"5 #$r$# )e)(a"#$ dala) pela!aa" e!e)p$r"aa" lap&ra" i"i* Ahir"7a pe"7$!$" )e"5harapa" !e)$a lap&ra" pra#i$) 7a"5 #elah di!$!$" i"i dapa# (er)a"


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LAPORAN PRAKTIKUM OPERASI TEKNIK KIMIA I FLUIDISASI UPN “VETERAN” JAWA TIMUR

DA-TAR ISI

LEMBAR PENGESA4AN************************************************************************************i KATA PENGANTAR *********************************************************************************************ii DA-TAR ISI**********************************************************************************************************iii INTISARI **************************************************************************************************************i= BAB I PENDA4ULUAN***************************************************************************************I.1 Latar B('aa&**********************************************************************************************I.2 Ta************************************************************************************************************4 I.3 Ma7aat**********************************************************************************************************4 BAB II TINAUAN PUSTAKA****************************************************************************0 II.1 S()ara U88***********************************************************************************************0 II.1.1 P(&(rtia S)r((i& ******************************************************************************0 II.1.2T(i P(&a#aa******************************************************************************0 II.1.3 Sta!ar P(&a#aa *****************************************************************************> II.1.9 8'a$ Parti(' Da'a8 :a8;ra****************************************************6 II.2 Si7at Ba$a ***************************************************************************************************. II.3 4i;*t("a******************************************************************************************************-1 II.9 Dia&ra8 A'ir**********************************************************************************************-BAB III PELAKSANAAN PRAKTIKUM********************************************************-4 III.1 Ba$a********************************************************************************************************-4 III.2 A'at************************************************************************************************************-4 III.3 Ga8+ar A'at*********************************************************************************************-4 III.9 Ra&aia A'at*****************************************************************************************-0 III.5 Pr*"(!r P(r)*+aa ********************************************************************************-0

Program Studi S-1 Teknik Kimia Fakultas Teknik-UPN “VETERAN”JAT!

iii



iv


INTISARI

Dala) pr&!e! i"d$!#ri )i!al"7a pada pe"5&laha" )a#erial (er$pa )i"eral* Mi"eral #er#e"#$ diperl$a" ada"7a pe"5a7aa"* Pe"5a7aa" a#a$ pe"7ari"5a" adalah pr&!e! pe)i!aha" !e9ara )ea"i erda!ara" $$ra" par#iel da" $"#$ )e"dapa#a" $$ra" par#iel 7a"5 !era5a)* Pada pr&!e! pe"5a7aa" ?a# pada# dile)par a#a$ di%a#$ha" e per)$aa" pe"5a7aa" 7a"5 )e)p$"7ai le(a"5 (er$$ra" #er#e"#$, ?a# pada# de"5a" $$ra" (e!ar aa" #er#i"55al da" ?a# pada# de"5a" $$ra" 7a"5 le(ih e9il dapa# )ele;a#i l$(a"5* Pr&!e! da" )e#&de pe"5a7aa" #elah die"al !e9ara l$a! 7a"5 dipaai dala) pr&!e! i"d$!#ri* Adap$"

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BAB I PENDA4ULUAN

I.1 Latar B('aa&

Opera!i #e"i i)ia )e)erl$a" pe"5a)a#a" !e9ara la"5!$"5 are"a (ere"aa" de"5a" pr&!e! pada peri!#i;a #e"i i)ia* Dala) pr&!e! i"d$!#ri )i!al"7a pada pe"5&laha" )a#erial (er$pa )i"eral* Mi"eral #er#e"#$ diperl$a" ada"7a pe"5a7aa"* Pe"5a7aa" a#a$ pe"7ari"5a" adalah pr&!e! pe)i!aha" !e9ara )ea"i erda!ara" $$ra" par#iel da" $"#$ )e"dapa#a" $$ra" par#iel 7a"5 !era5a)* Pada pr&!e! pe"5a7aa" ?a# pada# dile)par a#a$ di%a#$ha" e per)$aa" pe"5a7aa" 7a"5 )e)p$"7ai le(a"5 (er$$ra" #er #e"#$, ?a# pada# de"5a" $$ra" (e!ar aa" #er#i"55al da" ?a# pada# de"5a" $$ra" 7a"5 le(ih e9il dapa# )ele;a#i l$(a"5* Pr&!e! da" )e#&de pe"5a7aa" #elah die"al !e9ara l$a! 7a"5 dipaai dala) pr&!e! i"d$!#ri* Pada pr&!e! pe"5$$ra" ($#ira" pada#a" (er$pa pe"5a7aa"* La"5ah per#a)a adalah de"5a" )e"7iapa" a7aa" de"5a" $$ra" -1 )e!h, 01 )e!h, da" 21 )e!h, e)$dia" !iapa" (aha" !e!$ai =aria(el 7a"5 #elah di#e"#$a", lal$ a7a de"5a" a7aa" -1 )e!h, 01 )e!h, da" 21 )e!h* Ti)(a"5 )a!i"58)a!i"5 (aha" 7a"5 #er#aha" @&=er!i?e da" (aha" 7a"5 l&l&! @$"der!i?e, lal$ hi#$"5 ha!il per9&(aa" pr&!e"#a!e &=er!i?e da" $"der!i?e* Pada per9&(aa" i"i (er#$%$a" $"#$ )e)pela%ari pr&!e! da" )e#&de pe"5a7aa", $"#$ )e"dapa#a" ha!il pr&d$ !e!$ai de"5a" $$ra" 7a"5 dii"5i"a", $"#$ )e)i!aha" ?a# pada# !e$ai de"5a" $$ra" 7a"5 dii"5i"a", da" $"#$ )e"5e#ah$i

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I.2 Ta

-* U"#$ )e)pela%ari pr&!e! da" )e#&de pe"5a7aa"* 4* U"#$ )e)i!aha" ?a# pada# !e!$ai de"5a" $$ra"7a"5 dii"5i"a"* 0* U"#$ )e"dapa#a" ha!il !e!$ai de"5a" $$ra" 7a"5 dii"5i"a"* >*U"#$ )e"5hi#$"5 pr&!e"#a!e ?a# pada# 7a"5 #ida #er!ari"5 @&=er!i?e da" ?a# pada# 7a"5 #er!ari"5 @$"der!i?e * I.3 Ma7aat

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BAB II TINAUAN PUSTAKA II.1 S()ara U88 II.1.1 P(&(rtia S)r((i&

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02 @A"55rae"i, 411.


9


Me!h adalah $$ra" dari %$)lah l$(a"5 !$a#$ %ari"5 a#a$ a!a pada l$a!a" - i"9h per!e5i %ari"5  a!a 7a"5 (i!a dilal$i &leh )a#erial pada#* Me!h 41 )e)ili ar#i #erdapa# 41 l$(a"5 pada (ida"5 %ari"5  a!a !el$a! - i"9h, de)iia" !e#er$!"7a* U$ra" )e!h (a"7a di5$"aa" pada pr&!e! pe"ep$"5a" a#a$ pe"5hal$!a" !$a#$ (aha" pada#a", 7a"5 !e(el$) dihal$!a" )e)ilii $$ra" 7a"5 le(ih (e!ar* Pa(ri !e)e", #ep$"5 )aa"a", i"d$!#ri )e#al$r5i, da" pa(ri p&;der &!)e#i, )e"55$"aa" $$ra" )e!h dala) pr&!e! pr&d$!i"7a*

Tabel 2. Ukuran Mes ! in"i ! milimeter ! mikr#meter

M("$ 0 > 2 / 6 3 -1 -4 -> -/ -3 41 42 43 01 02 >1 >2 21

I)i 1*4/21 1*-361 1*-261 1*-041 1*---1 1*1.06 1*1636 1*1//1*1222 1*1>/. 1*10.> 1*1001*1431 1*1403 1*1404 1*1-.6 1*1-/2 1*1-03 1*1--6

Mi''i8(t(r /*601 >*6/1 >*111 0*0/1 4*301 4*031 4*111 -*/31 -*>-1 -*-.1 -*111 1*3>1*616 1*611 1*2.2 1*211 1*>41 1*02> 1*4.6

Mir*8(t(r /601 >6/1 >111 00/1 4301 4031 4111 -/31 ->-1 --.1 -111 3>616 611 2.2 211 >41 02> 4.6

@Be!#ei", 41-2 


1$


II.2 Si7at Ba$a

-* Pa!ir K$ar!a A* Si

11


Se)ai" e9il $$ra" l$(a"5 a7aa" )aa !e)ai" (a"7a (aha" 7a"5 #er#aha" dia#a! a7aa" *!eda"5a" !e)ai" (e!ar $$ra" l$(a"5 a7aa" )aa !e)ai" !dii# (aha" 7a"5 #er#aha" dia#a! a7aa"*


12


II.9 Dia&ra8 A'ir


13


BAB III PELAKSANAAN PRAKTIKUM III.1 Ba$a

-* Pa!ir $ar!a /11 5ra) III.2 A'at

-* A7aa" 4* L&7a"5 0* Nera9a a"ali#i III.3 Ga8+ar A'at

L&7a"5

Nera9a a"ali#i

A7aa" III.9 Ra&aia A'at P(r)*+aa

A7aa" 01 )e!h

A7aa" 21 )e!h

A7aa" /1 )e!h


Pe"a)p$"5

14


III.5 Pr*"(!r P(r)*+aa

-* Siapa" a7aa" (er$$ra" 01 )e!h, 21 )e!h, da" /1 )e!h* 4* Ti)(a"5 pa!ir $ar!a /11 5ra)* 0* A7a pa!ir $ar!a de"5a" a7aa" 01 )e!h, lal$ #i)(a"5 pa!ir 7a"5 #er#aha" @&=er!i?e* >* A7a par#iel $"der!i?e dari !9ree" $$ra" 01 )e!h de"5a" !9ree" $$ra" 21 )e!h da" #i)(a"5 pa!ir 7a"5 #er#aha" @&=er!i?e* 2* A7a par#iel $"der!i?e dari !9ree" $$ra" 21 )e!h de"5a" !9ree" $$ra" /1 )e!h lal$ #i)(a"5 pa!ir 7a"5 #er#aha" @&=er!i?e da" pa!ir 7a"5 l&l&! @$"der!i?e* /* Ci#$"5 ha!il per9&(aa" pre!e"#a!e &=er!i?e da" $"der!i?e*

BAB I 4ASIL DAN PEMBA4ASAN


15


I.1. Ta+(' 4a"i' P(&a8ata

Baha"

' Pa!ir K$ar!a

Ma!!a a;al Baha" Pa!ir K$ar!a

!6$$ %ram

Me!h 01 21 /1

T&#al

O=er!i?e 0-1 --1 -11 /11 5r

U"der!i?e 8 8 31

I.2. Ta+(' 4a"i' P(r$it&a !a P(r$it&a I.1.1 Ta+(' 4a"i' P(r$it&a : < 0.5233


16


Bera#

Me!h

A;al

J$)lah

Fra!i

Par#iel

Ma!!a @H

@N 01

1*2-/

D@i"

D0@i"0

Ma!!a Par#iel @5ra) /*62 H -1 8 > >

/11 5ra)

21 /1 /1

1*-30

4*4-

1*-//

-18/ -0*10H

1,-00

-186 -0*10H

1*..3

-186 /,6.3H

@$"der!i?e %$)lah

-18>

I.2.2. P(r$it&a -*Fra!i )a!!a

Fra!i )a!!a par#iel 

a* 01 )e!h




17

H

-3634


(* 21 )e!h



9* /1 )e!h



d* /1 )e!h



4*Fra!i )a!!a #&#al  &=er!i?e 01  &=er!i?e 21  &=er!i?e /1  $"der!i?e /1  1*2-6  1*-30  1*-/6  1*-00 0*Ma!!a Par#iel a* O=er!i?e pada !9ree" 01 )e!h

  4*/2H 1*2400 H >*36 H -1 8>  /*62 H -1 8> 5ra)

(* O=er!i?e pada !9ree" 21 )e!h

  4*/2H 1*2400 H -*/ H -1 8/  4*4- H -18/ 5ra)

9* O=er!i?e pada !9ree" /1 )e!h

  4*/2 H 1*2400 H .*> H -1 86  -0*10H -1 86 5ra)

d* O=er!i?e pada !9ree" /1 )e!h

  4*/2 H 1*2400 H .*> H -1 86  -0*10H -1 86 5ra)

>*J$)lah par#iel

Ni

<

a* 01 )e!h



(* 21 )e!h



9* /1 )e!h



d* /1 )e!h



J$)lah par#iel #&#al  &=er!i?e 01  &=er!i?e 21  &=er!i?e /1  $"der!i?e /1 Program Studi S-1 Teknik Kimia Fakultas Teknik-UPN “VETERAN”JAT!

18










-3634>-./*0 2*D a=era5e a* D a=era5e -  (* D a=era5e - 

/* TAAD



 4*06 H -1 86

6* Mea" S$r
<

<

1*10>

3* Mea" V&l$)e Dia)e#er @D=

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19


 1*1-I.3 Gra7i @Tida ada I.9 P(8+a$a"a

Per9&(aa"

pe"5$$ra"

($#ira"

(er#$%$a"

$"#$

)e)i!aha"

da"

)e"5el&)p&a" pada#a" !e!$ai $$ra" 7a"5 dii"5i"a"* Ca!il pe"5a7aa" aa" )e"5ha!ila" pr&d$ 7a"5 !era5a), 7a"5 !ela"%$#"7a dapa# dipr&!e! de"5a" pr&!e! 7a"5 lai"* Ca!il 7a"5 diper&leh aa" #er(a5i )e"%adi pada#a" 7a"5 #ida l&l&! !ari"5a" @&=er!i?e da" pada#a" 7a"5 l&l&! !ari"5a" @$"der!i?e* Pada pra#i$) i"i pra#ia" dapa# )e"e"#$a" 3*00, 01, da" -0*04* $"#$ pr&!e"#a!e pr&d$ &=er!i?e dari a7aa" 01 )e!h, 21 )e!h, da" /1 )e!h (er#$r$#8#$r$# adalah ' 2-*/0, -1*00, da" -/*/6*

2$


Pada pra#i$) i"i (erla$ "era9a )a!!a di)a"a )a!!a pa!ir $ar!a 7a"5 )a!$ da" el$ar !e(a"7a /11 5ra)* Jia ha!il 7a"5 didapa# $ra"5, hal #er!e($# dapa# (era!al dari e!alaha" pra#ia"* Dala) pra#i$) pe"5$$ra" ($#ira" pada#a" i"i ha!il &=er!i?e da" $"der!i?e %$5a dipe"5ar$hi &leh (e!ar8e9il"7a "ilai )e!h a#a$ $$ra" l$(a"5 7a"5 dipaai* Kadar air (aha" %$5a har$! diperha#ia" $"#$ )e)perla"9ar pr&!e! pe"5a7aa"*


21


BAB  KESIMPULAN DAN SARAN

.1. K("i8;'a

Berda!ara" per9&(aa"
-* Se(ai"7a pra#ia" Dala) )ela$a" pe"5a7aa" le(ih (erha#i8 ha#i a5ar (aha" #ida #erle)par el$ar dari a7aa"* 4* Se(ai"7a pra#ia" le(ih )e)aha)i #e&ri da" pr&!ed$r 7a"5 #erdapa# dala) pra#i$) pe"5$$ra" ($#ira" pada#a" !e(el$) )ela$a" pra#i$) 0 * S e( ai " 7a p ra # ia "

l e( ih

# el i# i

da "

( er & "! e" #r a! i

d al a)

pe "9 a# a#a" ha !i l da " )e la $ a" pe rh i# "5 a"


22


DA-TAR PUSTAKA

A"55rae"i,Ir)a D;i*411.*”METODE DAN TEKNIK PENGAAKAN UNTUK MENENTUKAN

UKURAN

PARTIKEL

DALAM

TEKNOLOGI

FARMASI”*@h##p'#!<

23

1. Pengukuran Butiran Padatan

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