H O W
T O
M A K E
C O C A I N E
********************************************************************** BROUGHT TO YOU BY: CUBE
1994-05-04
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141 " o& ,%.o3,l(m$e ,%.oclo.$%e+ He(t to .e&l#3 #t$l %$22ole% (%% 10< " o& (,%.o#2 2o%$#m c(./o(te $ 2m(ll !o.t$o2 (2 &(2t (2 .e(ct$o '$ll (llo'+ Re&l#3 &o. 64 o#.2 (% &$lte. te m$3t#.e+ E(!o.(te te &$lt.(te to %.,e22 #%e. (c#o+ T()e #! te .e2$%#e $ te m$$m#m (mo#t o& /o$l$" '(te. %ecolo.$@e '$t c(./o &$lte. (% (llo' to .ec.,2t(ll$@e $ .e&.$"e.(to.+ $lte. to "et !.o%#ct (% cocet.(te to "et (%%$t$o(l c.o!+ Y$el% o& 2#cc$(l%o3$me !o'%e. $2 ( l$ttle oe. 40 " m! $2 1;11;6*+ 5+> " o& te (/oe !o'%e. $2 !l(ce% $ ( /e()e. o& 650 ml c(!(c$t, (% 54 ml o& 10 2#l&#.$c (c$% $2 (%%e%+ Cool to 0* (% (%% $ 2m(ll !o.t$o2 o& ; " o& 2o%$#m $t.$te 7$& ,o# (%% te $t.$te too &(2t $t.o"e %$o3$%e &#me2 '$ll eole+ A&te. te %$o3$me $2 com!letel, %$22ole% (llo' te 2ol#t$o to '(.m to 60* (% e&&e.e2cece to "o to com!let$o+ Ne#t.(l$@e te ,ello' 2ol#t$o to l$tm#2 /, (%%$" 2m(ll !o.t$o2 o& /(.$#m c(./o(te+ $lte. o&& te /(.$#m 2#l&(te t(t !.ec$!$t(te2+ Te &$lt.(te $2 90 !#.e 2#cc$%$(l%e,%e (% $2 ot !#.$&$e% &#.te. &o. te .e(ct$o to c.e(te t.o!$oe+ o t$2 !.oce%#.e 8 mo.e t$me2 to "et te !.o!e. (mo#t &o. te e3t 2te! o. m#lt$!l, te (mo#t2 "$e /, &o#. (% !.ocee% (2 %e2c.$/e% (/oe+ T()e te tot(l (mo#t o& 2#cc$(l%e,%e 7o/t($e% &.om 4 o& te (/oe 2,te2e2 com/$e% (% '$to#t &#.te. t.e(tmet o. !#.$&$c(t$o 7t$2 (% /ette. /e 15+5 " o& 2#cc$%$(l%e,%e !#t $to ( E.leme,e. &l(2) o&
4-5 l$te.2 c(!(c$t,+ A%% 61+< " o& met,l(m$e ,%.oclo.$%e 4<+; " o& (cetoe%$c(./o3,l$c (c$% (% eo#" '(te. to m()e ( tot(l ol#me o& 6 l$te.2+ A%D#2t te !H to >-10 /, 2lo'l, (%%$" ( 2(t#.(te% 2ol#t$o o& %$2o%$#m !o2!(te+ Te co%e2(te o& t$2 .e(ct$o 7(llo' to 2et &o. (/o#t < %(,2 $2 e3t.(cte% '$t ete. te ete.e(l 2ol#t$o $2 %.$e% oe. 2o%$#m 2#l!(te (% %$2t$lle% te !.o%#ct com$" oe. (t 118* (t 65 mm o& !.e22#.e $2 collecte%+ U!o cool$" 14 " o& t.o!$oe c.,2t(ll$@e2 $ te !#.e 2t(te+ 6-C(./ometo3,t.o!$oe+ A m$3t#.e o& 1+85 " o& 2o%$#m meto3$%e 7t$2 $2 2o%$#m $ ( m$$m#m (mo#t o& met(ol 8+5 " o& t.o!$oe 4 ml o& %$met,lc(./o(te (% 10 ml o& tol#ee $2 .e&l#3e% &o. 80 m$+ Cool to 0* (% (%% 15 ml o& '(te. t(t cot($2 6+5 " o& (mmo$#m clo.$%e+ E3t.(ct te 2ol#t$o (&te. 2()$" '$t '$t &o#. 50 ml !o.t$o2 o& clo.o&o.m %., e(!o.(te te clo.o&o.m $ (c#o+ $22ole te o$l .e2$%#e $ 100 ml o& ete. '(2 t'$ce '$t ( m$3t#.e o& < ml o& 2(t#.(te% !ot(22$#m c(./o(te (% t.ee ml o& 8 N KOH+ ., (% e(!o.(te $ (c#o to .ecoe. te #.e(cte% t.o!$oe+ T()e #! te o$l $ ( 2ol#t$o o& (?#eo#2 (mmo$#m clo.$%e (% e3t.(ct '$t clo.o&o.m %., (% e(!o.(te $ (c#o to "et ( o$l+ Te o$l $2 %$22ole% $ ot (cetoe cool (% 2c.(tc $2$%e o& &l(2) '$t "l(22 .o% to !.ec$!$t(te 6-c(./ometo3,t.o!$oe+ Rec.,2t(ll$@e 1< " o& t$2 !.o%#ct $ 80 ml o& ot met,l (cet(te (% (%% 4 ml o& col% '(te. (% 4 ml o& (cetoe+ #t $ &.ee@e. &o. 6 16 to 8 o#.2+ $lte. (% '(2 te !.ec$!$t(te '$t col% met,l (cet(te to "et !#.e !.o%#ct+ Met,lec"o$e+ 0+4 mole o& t.o!$oe $2 2#2!e%e% $ >0 ml o& et(ol $ ( (.. ,%.o"e(t$o &l(2) 7o. 2omet$" t(t c( t()e 100 !2$ (% ot
.e(ct '$t te .e(ct$o l$)e 2t($le22 2teel o. "l(22+ 10 " o& R(e, N$c)le $2 (%%e% '$t "oo% ("$t(t$o 72t$..$" o. 2()$" &ollo'e% /, 6-8 ml o& 60 N(OH 2ol#t$o+ e(l e22el $t.o%#ce 50 !2$ o& ,%.o"e (tmo2!e.e 7(&te. &l#2$" e22el '$t ,%.o"e (% e(t to 40-50*+ A&te. o mo.e #!t()e o& ,%.o"e 7!.e22#.e "(#"e '$ll ol% 2te(%, (&te. %.o!!$" to $t2 lo'e2t !o$t /lee% o&& !.e22#.e (% &$lte. te $c)le o&& .$2e o#t /ottle '$t clo.o&o.m (% #2e t$2 .$2e to .$2e o&& te $c)le '$le 2t$ll o te &$lte. !(!e.+ M()e te &$lt.(te /(2$c '$t KOH (&te. cool$" to 10*+ E3t.(ct '$t clo.o&o.m %., (% e(!o.(te te clo.o&o.m $ (c#o to "et ( o$l+ M$3 te o$l !l#2 (, !.ec$!$t(te '$t ( e?#(l ol#me o& %., ete. (% &$lte.+ A%% mo.e %., ete. to te &$lt.(te #t$l o mo.e !.ec$!$t(te &o.m2 &$lte. (% (%% to te .e2t o& te !.ec$!et(te+ Rec.,2t(ll$@e &.om $2o!.o!(ol to "et !#.e met,lec"o$e+ Te2t &o. (ct$$t,+ I& (ct$e 2)$! %o' to te 2te! &o. coc($e+ I& ot (ct$e !.ocee% (2 &ollo'2+ t$. '$t (ct$(te% c(./o &o. 80 m$ &$lte. e(!o.(te $ (c#o %$22ole te /.o' l$?#$% $ met(ol (% e#t.(l$@e '$t 10 HCl (c$% $ %., ete.+ E(!o.(te te ete. #t$l te t'o l(,e.2 %$2(!!e(. (% (llo' to 2t(% &o. 6 o#.2 (t 0* to !.ec$!$t(te te t$tle !.o%#ct+ Te.e (.e m(, '(,2 to .e%#ce 6-c(./ometo3,t.o!$oe to met,lec"o$e+ I co2e to %e2$" ( R(e, N$c)le .e%#ct$o /ec(#2e $t $2 ce(! (% ot (2 2#2!$c$o#2 (2 FAH (% $t $2 m#c e(2$e. t( @$c o. 2o%$#m (m(l"(m2+ Coc($e+ 4+15 " o& met,lec"o$e (% 5+; " o& /e@o$c (,%.$%e $ 150 ml
o& %., /e@ee (.e "etl, .e&l#3e% &o. 4 o#.2 t()$" !.ec(#t$o ("($2t H60 7te 6 2o#l% /e o ( lo'e. leel $ te ($. 7%.,$" t#/e+ Cool $ ( $ce /(t (c$%$&, c(.e&#ll, '$t ,%.oclo.$c (c$% %., (% e(!o.(te $ ( (c##m to "et ( .e% o$l '$c $2 t.e(te% '$t ( l$ttle !o.t$o o& $2o!.o!(ol to !.ec$!$t(te coc($e+ A2 ,o# c( 2ee t$2 $2 ?#$te ( co.e+ Te coc( le(e2 "$e ec"o$e '$c (2 ,o# c( 2ee $2 ol, ( D#m! ('(, &.om coc($e+ I& ,o# c( "et e"co$e te %$22ole > 16 " o& $t $ 100 ml o& et(ol (% !(22 7/#//le %., HC1 "(2 t.o#" t$2 2ol#t$o &o. 80 m$+ Fet cool to .oom tem! (% let 2t(% &o. (ote. 1 16 o#.2+ Getl, .e&l#3 &o. 80 m$ (% e(!o.(te $ (c#o+ B(2$&, te .e2$%#e o$l '$t N(OH (% &$lte. to "et >+4 " o& met,lec"o$e '$c $2 coe.te% to coc($e (2 $ te coc($ 2te! (/oe+ Belo' $2 "$e ( 2ome'(t e(2$e. meto% o& !.o%#c$" t.o!$oe /, te "ee.(l meto%2 o& W$ll2t(tte. 'o '(2 $2t.#met(l $ te &$.2t 2,tet$c !.o%#ct$o o& coc($e (% 2ee.(l ote. (l)(lo$%2+ A&te. .e$e'$" t$2 meto% I &o#% $t to /e 2$m!le. t( te (/oe $ m(, .e2!ect2+ T.o!$oe+ 10 " o& !,..ol$%$e%$et,l %$(cet(te (.e e(te% '$t 10 " o& c,mee (% 6 " o& 2o%$#m !o'%e. te .e(ct$o t()$" !l(ce (t (/o#t 1<0*+ #.$" te .e(ct$o 7'$c $2 com!lete $ (/o#t 10 m$ te tem! 2o#l% ot e3cee% 1;6*+ Te .e2#lt$" .e(ct$o !.o%#ct $ %$22ole% $ '(te. te 2(t#.(te% '$t !ot(22$#m c(./o(te (% te o$l '$c 2e!(.(te2 $2 /o$le%
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;14 mm (c#o+ Te t.o!$oe2 c( /e #2e% $ te (/oe &o.m#l( 7o. $ ( &o.m#l( t(t ,o# (e &o#% el2e'e.e to /e coe.te% to coc($e+ Remem/e. to .ec.,2t(ll$@e te 6-c(./ometo3,t.o!$oe /e&o.e coe.t$" to met,lec"o$e+ ---------------------------------------------------------------------T$2 te3t $2 2!.e(% &o. $&o.m(t$o(l !#.!o2e ol,+ I (m ot .e2!o2$/le $& 2omeoe $2 $D#.e% '$le #2$" t$2 $&o.m(t$o+ A&te. (ll $&o.m(t$o '(t2 to /e &.ee+ ----------------------------------------------------------------------
