IDENTIFIKASI MERKURI PADA KOSMETIK
DOSEN PENGAJAR : DEWI SARI MULIA, M.Si., Apt SUSI NOVARYATIIN, M.Si MUHAMMAD RIZKI F.P, M.Si., Apt
ASISTEN DOSEN : SUNARDI, Amd.F!m GA"RILE NATASIA, Amd.F!m EMIE MAHDALENA, Amd.F!m
DISUSUN OLEH : KHAIRIANNUR (15.71.016745)
NIDYA
(15.71.016329)
RANI DI A.
(15.71.016325)
MIRNAATI
(15.71.016332)
NO!I NO!IT TA SAR SARII
(15. (15.71 71.0 .016 1692 923) 3)
PRO"RAM STUDI D#III FARMASI FAKULTAS AKULTAS ILMU ILM U KESE KESEHAT HATAN AN UNI!ERSITAS MUHAMMADIYAH PALAN"KARAYA 2017
DAFTAR ISI
JUDUL...................................................................................................................................i DAFTAR ISI.........................................................................................................................ii I.
T#$# T#$#%.. %...... ....... ...... ....... ....... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ......... .......... ......& .&
II.
D'! T()!i.......................................................... ............................... .............. ........ ......& &
III. IV. IV.
A*t + "%......... "%............... ............. .............. .............. ............. ............. .............. .............. ............. ............. .............. ............. ............. ...............P!)'(d#! P!)'(d#! K(!$....... K(!$.............. ............. ............. .............. .............. ............. ............. .............. ............. ............. .............. .................. ................. ......
V.
H'i* H'i* P(%/m P(%/mt% t%.... ....... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ....... ......... ........0 ...0
VI.
P(m1'%... P(m1'%.......... ............. ............. .............. ............. ............. .............. .............. ............. ............. .............. .............. ...................... ..................2 ...2
VII.
K('imp#*%. K('imp#*%........ ............. ............. .............. ............. ............. .............. .............. ............. ............. ................... ................................3....................3-
VIII. VIII.
D4t! D4t! P#'t5.. P#'t5........ ............. .............. .............. ............. ............. .............. ............. ............. .............. .............. ...................... ....................3 .....3
I6.
Lmpi! Lmpi!%.. %..... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ......... .......... .......... .......... ......... ........30 ....30
3
DAFTAR ISI
JUDUL...................................................................................................................................i DAFTAR ISI.........................................................................................................................ii I.
T#$# T#$#%.. %...... ....... ...... ....... ....... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ......... .......... ......& .&
II.
D'! T()!i.......................................................... ............................... .............. ........ ......& &
III. IV. IV.
A*t + "%......... "%............... ............. .............. .............. ............. ............. .............. .............. ............. ............. .............. ............. ............. ...............P!)'(d#! P!)'(d#! K(!$....... K(!$.............. ............. ............. .............. .............. ............. ............. .............. ............. ............. .............. .................. ................. ......
V.
H'i* H'i* P(%/m P(%/mt% t%.... ....... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ....... ......... ........0 ...0
VI.
P(m1'%... P(m1'%.......... ............. ............. .............. ............. ............. .............. .............. ............. ............. .............. .............. ...................... ..................2 ...2
VII.
K('imp#*%. K('imp#*%........ ............. ............. .............. ............. ............. .............. .............. ............. ............. ................... ................................3....................3-
VIII. VIII.
D4t! D4t! P#'t5.. P#'t5........ ............. .............. .............. ............. ............. .............. ............. ............. .............. .............. ...................... ....................3 .....3
I6.
Lmpi! Lmpi!%.. %..... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ....... ...... ....... ....... ....... ....... ...... ....... ....... ...... ....... ......... .......... .......... .......... ......... ........30 ....30
3
I.
TU$UAN . M(%/(t#i M(%/(t#i 4#%/'i id(%ti4i5' id(%ti4i5'ii m(!5#!i m(!5#!i pd 5!im 5!im 5)'m(ti5. 5)'m(ti5. 1. M(%/(t#i 1t' 5%d#%/% m(!5#!i pd 5!im 5)'m(ti5. 7. Mmp# m(*5#5 m(*5#5% % (5't!5'i (5't!5'i *)/m 1(!t 1(!t m(!5#!i m(!5#!i d*m 'mp(* 'mp(* 5)'m(ti 5)'m(ti5. 5. d. M(mp# M(mp# m(*5#5% m(*5#5% #$i id(%ti4i id(%ti4i5' 5'ii m(!5#! m(!5#!ii d(%/% d(%/% m(t)d( m(t)d( !(5'i 8!%, 8!%, p(%/(%dp%, '(!t p(m1(%t#5% m*/m.
II.
DASAR TEORI
K#*it p#ti d% 7(! m(!#p5% dm1% '(tip )!%/, t(!#tm 5#m 8%it. O*( 5!(% it# '(tip )!%/ 1(!#' #%t#5 m(%$/ d% m(mp(!1i5i 5('( 5('(t t% % 5#*i 5#*it% t%9 9 '(i '(i%// %// 5(1% 5(1%9 95% 5% 5#m 5#m 8%i 8%it t '(* '(**# *# 1(!# 1(!#' ' 1(!p(%mpi*% m(%!i5. H* i%i did#5#%/ p#* d(%/% '(m5i% 1(!5(m1%/%9 t(5% t(5%)* )*)/i )/i p(! p(!8 8t t% % 5#*it 5#*it d% d% 5*i% 5*i%i5 i55* 5*i%i i%i5 5 5(7% 5(7%ti ti5 5% % 9%/ 9%/ t(!' t(!'(1 (1!! di I%d)%('i. P(!8t% 5#*it t(* m(%$di t!(%d m' 5i%i 1/i 8%it m)d(!% d% m(!#p5% '(1# 5(1#t#% 1/i '()!%/ 8%it T)!m4(*dt + ")#!%(, 3;&;<. K#*it m(!#p5% 1/i% t#1# p*i%/ #tm 9%/ p(!*# dip(!ti5% 5!(% m(!#p5% )!/% t(!1('! 9%/ m(*pi'i 1/i% t#1# m%#'i. K#*it m(mi*i5i 4#%/'i #%t#5 m(*i%d#%/i 1/i% t#1# d!i 1(!1/i /%//#% d% !%/'%/% *#! d(%/% m(m1(%t#5 m(5%i'm( 1i)*)/i' '* 't#%9 9it# p(m1(%t#5% pi/m(% m(*%i% #%t#5 m(*i%d#%/i 5#*it d!i 19 'i%! #*t!=i)*( #*t!=i)*(tt mt!i. mt!i. Rdi'i Rdi'i 'i%! #*t!=i)*(t #*t!=i)*(t 9%/ 1(!'* 1(!'* d!i mt!i dpt m(%im1#*5% m(%im1#*5% (4(5 %(/ti4 %(/ti4 9it# m(%9(115% 1(!1/i p(!m'*% p(!m'*% pd 5#*it. "9 9%/ ditim1#*5% 9it# 5(*i%% 5#*it m#*i d!i 5(m(!%, %)d>%)d itm, p(%#% di%i, 5(5(!i%/%, 5(!ip#t, 'mpi 5%5(! 5#*it. U%t#5 m(%/t m(%/t'i 'i 1(!1/ 1(!1/i i m'* m'* 5#*it 5#*it t(!'(1 t(!'(1#t #t dip(!* dip(!*#5% #5% d%9 d%9 p(!8t p(!8t% % m(%//#%5% 5)'m(ti5 K#'%tti, 3;&-<.
&
K)'m(ti5 d* 1% t# '(di% 9%/ dim5'#d5% #%t#5 di/#%5% pd 1/i% *#! t#1# m%#'i. K)'m(ti5 't i%i '#d m(%$di 5(1#t#% p(%ti%/ 1/i m%#'i, 5!(% p(%//#%%%9 '(**# di/#%5% '(7! !#ti% d% t(!#'>m(%(!#'. T#$#% #tm p(%//#%% 5)'m(ti5 pd m'9!5t m)d(!% d* #%t#5 5(1(!'i% p!i1di, m(%i%/5t5% d9 t!i5 m(**#i m5(>#p, m(%i%/5t5% !' p(!79 di!i d% p(!'% t(%%/, m(*i%d#%/i 5#*it d% !m1#t d!i 5(!#'5% 'i%! #*t! =i)*(t, p)*#'i d% 45t)! *i%/5#%/% 9%/ *i%, m(%7(/ p(%#%, d% '(7! #m#m m(m1%t# '('()!%/ *(1i m(%i5mti d% m(%/!/i id#p K#'%tti, 3;&-<. P(%//#%% 5)'m(ti5 !#' di'('#i5% d(%/% t#!% p5i%9. Mi'*%9 !#' '('#i $(%i' 5#*it, 8!% 5#*it, i5*im, 7#7, 85t# p(%//#%%, #m#! d% $#m* p(m5i%%9 '(i%// tid5 m(%im1#*5% (4(5 9%/ tid5 dii%/i%5%. S(1(*#m m(mp(!/#%5% 5)'m(ti5, '%/t* p(%ti%/ #%t#5 m(%/(t#i *(1i d#*# p 9%/ dim5'#d d(%/% 5)'m(ti5, m%4t d% p(m5i% 9%/ 1(%!. M5 d!i it# p(!*# p(%$(*'% *(1i t(!p(!i%7i m(%/(%i 5)'m(ti5 D$$di''t!, 3;;<. "%95 pi*i% p!)d#5 5)'m(ti5 '* 't#%9, 9it# 5!im p(m#ti 8$ Wit(%i%/ ?!(m<. K!im p(m#ti m(!#p5% 7mp#!% 1% 5imi d% t# 1% *i%%9 d(%/% 5'it 1i' m(m#ti5% 5#*it t# m(m#7t5% %)d itm pd 5#*it. K!im p(m#ti '%/t 1(!m%4t 1/i 8$ 9%/ m(mi*i5i 1(!1/i m'* di 8$, 5!(% mmp# m(%/(m1*i5% 5(7(!% 5#*it d% m(%/#!%/i 8!% itm pd 8$ P!(%/5#%,3;&@<. "% 5ti4 9%/ 1i'%9 di/#%5% d*m 5!im p(m#ti '* 't#%9 d* m(!5#!i. M(!5#!i di'(1#t $#/ i! !5' t# 9d!!/9!#m 9%/ m(!#p5% (*(m(% 5imi d(%/% 'im1)* H/ d% t(!m'#5 d*m /)*)%/% *)/m 1(!t d(%/% 1(%t#5 7i! d% 1(!8!% 5(p(!5%. M(!5#!i m(!#p5% '* 't# 1% 5ti4 9%/ '(!i%/ ditm15% d*m 5!im p(m#ti. M(%#!#t D!. R(t%) I.S T!%//)%), Sp.KK m(!5#!i di!(5)m(%d'i5% '(1/i 1%
3
p(m#ti 5#*it 5!(% 1(!p)t(%'i '(1/i 1% p(!(d#5'i p(m#7t< 8!% 5#*it d(%/% d9 p(m#ti t(!dp 5#*it 9%/ '%/t 5#t. I)% m(!5#!i di%//p dpt
m(%/m1t 'i%t('i'
m(*mi% pi/m(% 5#*it di '(* m(*%)'it
Li W%/ %d H)%/ Z%/, 3;&&<.
M(%#!#t P(!t#!% "d% P(%/8' O1t d% M5%% R(p#1*i5 I%d)%('i %)m)! HK.;@.;&.3@.;.&&.0003 t#% 3;&& p(!'9!t% *)/m 1(!t $(%i' m(!5#!i H/< d* tid5 *(1i d!i & m/B5/ t# &m/BL &ppm<. H* t(!'(1#t t(!$di *%/'#%/
5!(% '(%98 m(!5#!i 5% 5)%t5 d(%/% 5#*it '(7!
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m(%/5i1t5% !(5'i i!it'i 9%/ 1(!*%/'#%/ 7#5#p 7(pt di%t!%9 dpt m(m1#t 5#*it t(!15!, m(%$di itm, d% 15% dpt 1(!5(m1%/ m(%$di 5%5(! 5#*it. Pd p(m5i% d)'i' ti%//i dpt m(%9(115% 5(!#'5% p(!m%(% )t5, p!#>p!#, /i%$*, m(%//%/# p(!5(m1%/% $%i%, '(!t dpt m(%im1#*5% m%i4('t'i /($* 5(!7#%% pd 'i't(m '!4 1(!#p /%//#% p(%/*it%, t!(m)!, i%')m%i, 5(pi5#%%, d% /(!5% t%/% m(%$di 1%)!m* t5'i<"POM RI, 3;&&<. M(%#!#t
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--BMENKESBPERBVB&22C t(%t%/ 1%, t 8!%, '#1't!t, t p(%/8(t d% t1i! '#!9 pd 5)'m(ti5. D*m 5d! 9%/ '(di5itp#% m(!5#!i dpt 1(!'i4t !7#%. M#*i d!i p(!#1% 8!% 5#*it, 1i%ti5>1i%ti5 itm, *(!/i, i!it'i, '(!t pd p(m5i% d)'i' ti%//i dpt m(%9(115% 5(!#'5% p(!m%(% )t5, /i%$* d% /%//#% p(!5(m1%/% $%i%. "5% pp!% $%/5 p(%d(5 d*m d)'i' ti%//i dpt m(%9(115% m#%t>m#%t, di!( d% 5(!#'5% p!#>p!# '(!t m(!#p5% t 5!'i%)/(%i5 "POM RI, 3;;<. P(%//#%% 5!im 5)'m(ti5 '(!t 5)mp)'i'i t 1(!19 9%/ t(!5%d#%/ di d*m '(di% '#t# 5!im 5)'m(ti5 p(!*# dip(!ti5%. K!(% p1i* di/#%5% d*m $%/5 85t# p%$%/ d% 1(!*(1i% di58ti!5%
@
dpt m(m195% 5('(t%. D(%/% *t! 1(*5%/ t(!'(1#t m'i'8 F!m'i U%i=(!'it' M#mmdi9 P*%/5!9 di1(!i5% mt(!i p!5ti5#m p(%/#$i% 5!im 5)'m(ti5 d(%/% $#d#* Id(%ti4i5'i M(!5#!i Pd K)'m(ti5 dim% 'mp(* dim1i* d!i p(%$#*>p(%$#* 5)'m(ti5 di5)t P*%/5!9.
III. ALAT DAN %AHAN A&'
&. T1#%/ !(5'i 3. R5 T1#%/ R(5'i @. Pip(t t(t(' -. ?8% p)!'(*i% . E!*(%m(9(! &;; mL 0. G(*' #5#! &; mL . L1# #5#! ; mL C. Tim1%/% %*iti5 2. H)t p*t( &;. "t%/ p(%/d#5 %''*
&. 3. @. -. . 0.
Smp*( K!im 5)'m(ti5 K(**9< Et(! ?3H<3O H?* 3 KI ;, N HNO@ P(5t A#'d('t
&&. &3. &@. &-. &. &0. &. &C.
"t%/ t(m1/ Amp*' Pip(t #5#! 3 mL d% & mL "** Pip(t ")t)* '(mp!)t K(!t' S!i%/ ?)!)%/ Pi' 3; mL G(*' "(5(! &;; mL
-
I!.
PROSEDUR KER$A A. P+,-'/'* L','*
P(m1#t% *!#t% KI ;, N K*i#m *)did dim1i* '(1%95 3 /!m, 5(m#di% di m'#55% 5( d*m *1# #5#! 3 mL d% ditm15% #d('t 'mpi t%d 3 mL, '(!t di5)7)5 i%// )m)/(% "#9#%/, 3;&&<.
P(m1#t% *!#t% # !$B# !(/i H?I P(5t dim1i* '(1%95 mL, 5(m#di% di m'#55% 5( d*m *1# #5#! &;; mL d% ditm15% d(%/% HNO@ P(5t '(1%95 3 mL p(!1%di%/% =)*#m @ : I< HAM M#*9)%), 3;;2<.
%. P,+/','-E-,'- S'/+& ('* 2005)
Tim1%/ 'mp(* 5#!%/ *(1i /!m, 5(m#di% 'mp(* dim'#5% 5(d*m 7)!)%/ pi', '(t(* it# (5't!5'i d(%/% 3; mL (t(!, 5)7)5 5#t i%// )m)/(% **# 1#%/ 4'( (t(! '(7! p(!*%.
P%'5% i%// 'mp(* mpi! 5(!i%/, 4'( ditm1 &; mL 7mp#!% 'm 5*)!id p(5t d% d% 'm %it!t p(5t @ : &<, 5(m#di% Up5%
di t' p(%%/' 'mpi mpi! 5(!i%/ Tm15% &; mL #d('t, didi5% '(1(%t!, di%/i%5%, d% '!i%/. . P+*'* +,, (H) (S8+&' 1990) 1. U A'&' Dim1i* *!#t% 'mp(*, m'#5% 5(d*m t1#%/ !(5'i, 5(m#di%
mp*' 1t%/ t(m1/ 'mpi m(%/5i*p, **# 7(*#p5% 5( d*m *!#t% #$i #%t#5 1(1(!p 't, $i5 p)'iti4 m(%/%d#%/ m(!5#!i m5 1t%/ t(m1/ 5% di*pi'i 1(!75 1#>1# m(%/5i*p. P%'5% pd %9* pi 1(1', 8!% 1#>1# 5% i*%/. 2. U U ,+'- ',*' +*'* '& ;' (KI) M'#55% 5( d*m t1#%/ !(5'i *!#t% 'mp(*, 5(m#di% ditm15% 3 t(t(' *!#t% K*i#m *)did ;, N p(!*% m(**#i di%di%/ t1#%/ !(5'i. H!#' tid5 t(!$di (%dp% $i%//, $i5 t(!$di (%dp% $i%// m5 p)'iti4 m(%/%d#%/ m(!5#!i.
!.
HASIL PEN"AMATAN A.
H'-& P+*'''* 1. H'-& P,+/','- S'/+& K;-+' (K+&&<) N O &.
SAMPEL
PERLAKUAN
HASIL
,&; /!m 5!im K(**9
3 mL Et(!
K#%i%/ '#'#
H?* 3 HNO@ P(5t P(!1%di%/ @:&< &; mL
K#%i%/ '#'#
Dip%'5% Hi%// Hmpi! 5(!i%/
K#%i%/ '#'#
A#d('t &; mL
P#ti K(5#%i%/%
Di'!i%/
P#ti '#'#
2. H'-& P+*'* S'/+& K;-+' (K+&&<) N O 1
2
PROSEDUR KER$A L!#t% #$i di7(*#p5% 1t%/ t(m1/ L!#t% #$i ditm15% 3 t(t(' *!#t% KI ;,N
HASIL
= #
"t%/ t(m1/ t(tp 1(8!% $i%// 5(m(!% ><
>
Tid5 d (%dp% d% *!#t% 1(!8!% 5#%i%/ ><
>
HASIL
= #
"t%/ t(m1/ 1(!#1 8!% m(%$di 1#>1# m(%/5i*p <
T(!dpt (%dp% m(! $i%// <
HASIL
= #
3. H'-& D'' K;*,;& P;-> N O 1
2
PROSEDUR KER$A L!#t% #$i di7(*#p5% 1t%/ t(m1/ L!#t% #$i ditm15% 3 t(t(' *!#t% KI ;,N
4. H'-& D'' K;*,;& P;-> N O
PROSEDUR KER$A
1
2
L!#t% A#d('t 3 mL di7(*#p5% 1t%/ t(m1/ L!#t% A#d('t & mL ditm15% 3 t(t(' *!#t% KI ;,N
"t%/ t(m1/ t(tp 1(8!% $i%// 5(m(!% ><
>
Tid5 d (%dp% m(! $i%// ><
>
5. H'-& D'' K+&'U A'&' +*'* %''* T+?''
KEL .
NAMA PRODUK
1.
?it! L'ti%/ ?))* S%)8<
2.
Fi! + L)=(*9
3.
K+&&< (K, S'/+& K+&. 3)
4.
G!%i(! S5#! Wit(
5.
D!. P#!(
6.
W!d
7.
T)p'9%
@.
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9.
Mi)% Vi7#m
10.
?)*/(%
U$I AMAL"AM DEN"AN %ATAN" TEM%A"A I
II
Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< $*' ++,''* (' '?#'? +*&'/) Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p<
Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< $*' ++,''* (' '?#'? +*&'/) Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p< Ji%// 5(m(!% tid5 1#>1# m(%/5i*p<
T(!1(%t#5 1#> 1# m(%/5i*p
T(!1(%t#5 1#> 1# m(%/5i*p
=#
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11.
L(#p!
12.
Nt#!* 22
Ji%// 5(m(!% tid5 1#>1# m(%/5i*p<
Ji%// 5(m(!% tid5 1#>1# m(%/5i*p<
(#)
T(!1(%t#5 1#> 1# m(%/5i*p
T(!1(%t#5 1#> 1# m(%/5i*p
(=)
U D+*'* KI
KEL .
NAMA PRODUK
U$I DEN"AN KI 05N
=#
I
II
1.
?it! L'ti%/ ?))* S%)8<
L!#t% "(!8!% K#%i%/
L!#t% "(!8!% K#%i%/
(#)
2.
Fi! + L)=(*9
L!#t% "(!8!% K#%i%/
L!#t% "(!8!% K#%i%/
(#)
3.
K+&&< (K, S'/+& K+&. 3)
L','* %+,',*' K**
L','* %+,',*' K**
(#)
4.
G!%i(! S5#! Wit(
L!#t% "(!8!% K#%i%/
L!#t% "(!8!% K#%i%/
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5.
D!. P#!(
L!#t% "(!8!% K#%i%/
L!#t% "(!8!% K#%i%/
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6.
W!d
L!#t% "(!8!% K#%i%/
L!#t% "(!8!% K#%i%/
(#)
7.
T)p'9%
L!#t% "(!8!% K#%i%/
L!#t% "(!8!% K#%i%/
(#)
@.
"19 Pi%5i''
L!#t% "(!8!% K#%i%/
L!#t% "(!8!% K#%i%/
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9.
Mi)% Vi7#m
L!#t% "(!8!% K#%i%/
L!#t% "(!8!% K#%i%/
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RANI DI APRILIAH (15.71.016325)
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NIDYA (15.71.016329)
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MIRNAATI (15.71.016332)
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NO!ITA SARI (15.71.016923)
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