Tribal Meth Webinar Series
Thursday, February 23, 2012
One‐Pot (Shake & Bake) Methamphetamine Labs
What This Presentation Is… Brief overview overview of of one one‐pot methamphetamine labs • Brief of some some of of their their hazards • Description of
• Lab identification
What This Presentation Is Not • This is not training on how to take down and process a meth lab! – To process a meth lab, you need a 40 hour Hazwopper class. If If your your agency sends you out to process a meth lab without this training and you get injured, your agency has some real liability problems.
– First Responder training is an 8‐hour course.
Dwain Worley - One Pot Method
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Tribal Meth Webinar Series
Thursday, February 23, 2012
One‐Pot labs convert pseudoephedrine into methamphetamine
One‐Pot Labs are a derivative of the Nazi method
Nazi Labs • Three Key Ingredients – Ephedrine/Pseudoephedrine – Lithium metal (Photo Batteries) – Sodium metal works also, but is rarely used.
– Anhydrous Ammonia
Dwain Worley - One Pot Method
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Tribal Meth Webinar Series
Thursday, February 23, 2012
Law Enforcement Targets Anhydrous Ammonia • Non‐approved Container Law • Stake out CO‐OP fertilizer lots • Tank Locks, Additives to Anhydrous to prevent synthesis, Dyes to Anhydrous tanks
DIY Anhydrous Ammonia Ammonium Nitrate or Ammonium Sulfate +
Sodium Hydroxide (Red Devil Lye) +
(a little) water = “Anhydrous” Ammonia
Ammonium Nitrate Cold Packs (gets cold when mixed with water) Urea based cold packs sort of work – but not very well.
Dwain Worley - One Pot Method
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Tribal Meth Webinar Series
Thursday, February 23, 2012
Ammonium Nitrate
Clandestine cooks are starting to use fertilizer sticks in place of the cold packs.
Obtaining Pseudoephedrine
Obtaining Pseudoephedrine Some states are controlling and/or monitoring the sale of pseudoephedrine.
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Tribal Meth Webinar Series
Thursday, February 23, 2012
Preparing Pseudoephedrine Tablets
Tablets are ground up, and occasionally extracted with solvent.
Obtaining Lithium
Lithium is removed from readily available “Lithium” batteries.
Obtaining Lithium
“Peeled” battery
Lithium is metal strip in front.
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Tribal Meth Webinar Series
Thursday, February 23, 2012
One‐Pot Methamphetamine Production Camp stove fuel is most common in Kansas. Starting fluid is often used as a solvent for the reaction. Starting fluid if very flammable.
One‐Pot/Shake & Bake • All ingredients (including flammable solvents, lithium and a small amount of water are added to a single container NOTE: Lithium reacts violently when it comes into contact with water
One‐Pot/Shake & Bake • After reaction takes place, the methamphetamine will be in the liquid layer.
• The liquid is “gassed” to obtain methamphetamine.
Dwain Worley - One Pot Method
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Tribal Meth Webinar Series
Thursday, February 23, 2012
HCl Gas Generators Salt and sulfuric acid drain cleaner are mixed to produce hydrogen chloride (HCl) gas. “Ice‐melt” products are sometimes substituted for rock salt.
“One‐Pot Gassing”
HCl gas from gassing generator is bubbled through the solvent / methamphetaminesolution to form methamphetamine crystals which …
“One‐Pot Gassing”
… falls to the bottom of the solution.
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Tribal Meth Webinar Series
Thursday, February 23, 2012
Methamphetamine Production
The solvent containing methamphetamine is filtered to recover the methamphetamine
One‐Pot Cook Video
NES / Tulsa PD “Experiments”
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Tribal Meth Webinar Series
Thursday, February 23, 2012
Pressure builds which limits reaction – until pressure is released. NOTE: Flashes of flame in right picture as lithium contacts water – insufficient oxygen to support flame.
Hot Lithium burns hole in bottom of plastic jar. Once released, sufficient oxygen is present to support flame.
Hot Lithium burns hole in bottom of plastic jar. Once released, sufficient oxygen is present to support flame.
Technically – this is not an explosion!
Dwain Worley - One Pot Method
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Tribal Meth Webinar Series
Thursday, February 23, 2012
NES / Tulsa PD “Experiments” • Eight (8) cooks were conducted – Four (4) cooks failed due to the reaction of lithium and water happening too close to the side of the bottle
– Of those four (4), three (3) burned through then had no additional flame/fire – One (1) of those four (4) did continue to burn after the bottle had failed
• In this case, it was not immediately after the failure. • In other states, cooks are using glass bottles and/or metal cans instead of plastic bottles ‐ these fail as well for the same reasons.
One‐Pot Hazards • Pressurized Bottles – Because pressure shuts down the reaction – a bottle can look pretty tame, but when the lid is cracked open the reaction can start up again.
– Pressurized solvents can spray out of the bottle. • This liquid can contain quite a bit of ammonia. • This liquid may contain lithium and water that can react and serve as an ignition source.
One‐Pot Hazards (continued)
• Rolling or tilting the bottle can expose un‐reacted lithium to water which can burn through the side of the container – causing flame thrower effect.
• Dried reaction material is fine strongly basic powder that can easily become airborne.
• Tulsa seems to have a lot of fire problems.
Dwain Worley - One Pot Method
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Tribal Meth Webinar Series
Thursday, February 23, 2012
Tulsa PD procedure (this is a summary – check with them for specifics)
• Get the Fire Department on scene • Wear appropriate safety gear • Wait until bottle starts reacting. • If necessary move bottle to safe area (outside) – Place in fire resistant over pack and pour Vermiculite around it.
– Once in safe area – remove from over pack • (working with over pack can produce chimney effect)
Tulsa PD procedure • Loosen lid slowly – if reaction starts up – back off and wait. – Repeat until cap is completely removed. • Use razor knife to cut off the top of container. • Scoop out floating lithium strips (don’t push them to the bottom). Place in mineral oil. • Pour off solvent. • Dispose of sludge.
One Pot Lab Evidence
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Tribal Meth Webinar Series
Thursday, February 23, 2012
One Pot Lab Evidence
(one man’s trash…)
One‐Pot Lab Evidence
One Pot Lab Evidence
Dwain Worley - One Pot Method
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Tribal Meth Webinar Series
Thursday, February 23, 2012
Common Hazards Of All Clandestine Labs • Inhalation And Splash Hazards – Strong Acids And Bases – Acid Gas Generators – Organic Solvents – Chemical Contamination
• Methamphetamine Cooks – Do Not Know The Chemical Dangers – Do Not Care About The Dangers
Current Trends • About 90% of what our KBI agents are getting is One‐Pot labs. • The other 10% depends on location – Southeast Kansas – mostly Red Phosphorus – Other places in Kansas – traditional Nazi
Cleanup Issues • When law enforcement executes a warrant on a meth lab, they are considered the generator of the hazardous waste.
• Funding for waste disposal & cleanup has become scarce.
• The appropriate time to address clan lab clean up is now – before you are on site wondering what to do with all of the hazardous material.
Dwain Worley - One Pot Method
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Tribal Meth Webinar Series
Thursday, February 23, 2012
Cleanup Issues • At one time KDHE helped with disposal of the chemicals. It was done right and in the most economical way possible. This was a something that Kansas did very well!
• KDHE also made sure that dwellings used as clan labs were safe before they could be reoccupied.
Questions?
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