Process Process Data Sheet
Cover / d n a n o i t a n i m e s s i d , n o i t c u d o r p e r o t d e t i
n i d e z i r o h t u a y l s s e r p x e s s e l n u d e t i b i h o r p m y i l l t t c o i r n t s t u e b r g a s n t i d n e u t l c n n o i c , n t s o i i t d a n z i a l i t t u n e r e m h u t o c o r o d / s d i n h t a f n o , o i t n a i o t i t o u l p b i r x t e i s y d n r A o
y r a t e i r p o r p l l a o t d e t i m i l t o n t u b g n i d u l c n i , s t h g i r l l A . s e g a m a d r o f e l b a i l e r a s r e d n e f f O . i g r u L y b g n i t i r w
. d e v r e s e r e r a , s t h g i r y t r e p o r p l a i r t s u d n i r e h t o r o / d n a s l e d o m y t i l i t u , s t n e t a p o t n o i t a l e r n i s t h g i r
06-T-0101 Ammonia Ammonia Scrubber I
CONFIDENTIAL Index of Revisions
a 0 . v e R
s l x . t e e h S r e v o C S D s s e c o r P i g r u L
00
All
PuW a
04/10/2015
Revision
Sheet
Name
Date
Prepared, Revis ed
Pr oject Nam e Case-Name:
Normal Case
DiS
CS
Nam e
Nam e
Checked
04/10/ 2015
IFI
Date
Status
Issued for Information Remark, kind of revision
Approved
Project No.
Docum ent No.
She et / of 1 / 7
Printed by / date / time:
Q.L. Revision 00 /
/
Process Process Data Sheet
Column-Reactor Sections n i d e z i r o h t u a y l s s e r p x e s s e l n u d e t i b i h o r p m y i l l t t c o i r n t s t u e b r g a s n t i d n e u t l c n n o i c , n t s o i i t d a n z i a l i t t u n e r e m h u t o c o r o d / s d i h n t a f n o , o i n t a i o t i t o u l b p i r x t e i s y d n r A o / d n a n o i t a n i m e s s i d , n o i t c u d o r p e r o t d e t i
y r a t e i r p o r p l l a o t d e t i m i l t o n t u b g n i d u l c n i , s t h g i r l l A . s e g a
01 Item Number
06-T-0101
02
. d e v r e s e r e r a , s t h g i r y t r e p o r p l a i r t s u d n i r e h t o r o / d m n a a d l s r e o d f e o l b m a y i t l i l i e t r a u , s t s r e n e d t n a e p f f o O t . i n g o r i u t a L l e r y b n i g s n t i t h i r i g w r
06
Unit Number
03
Unit Name
Rectisol
Designation
Ammonia Scrubber I
04 1
05 Number required
vertical
06 Orientation 07 Total volume
ft³
08 Total height
ft
24
09 10 Cyclic loading 11
Column Sections
12 Section number 13 Section description BFW, Raw Gas
14 Medium ft³
15 Volume 16 Height
ft
24
17 Inner diameter
in
134
lb/ft³
18 Density 19 Op. temp. max. / min.
°F
20 Op. pres. max. / min.
psi [a]
21 Des temp. max./min./vac. 22 Des pres. max./min./vac.
104
/
50
/
/
/
829.0
/ 3
807.6
/
/
/
°F
300 / 1000.> psi[g] /
/ CO2,H2S,COS,HCN,NH>
23 Corrosive components 24 Sour gas service (acc. Lurgi Std. Spec.) psi [a] 25 H 2 -partial pressure
/
/
/
/
/
/
/
/
/
/
/
/
aCAT3 444.31
@ 50 SS 316L
26 Material 27 Corrosion allowance
/
0.0
°F
@
°F
@
°F
@
°F
mm
28 Lining 29 Cladding No
30 Heat treatment 31
Process Internals 4 /
32
Bubble cup trays
/
/
/
/
/
/
SS 316L
33 34 1 /
35
Demister Wire Mesh SS316L
36 37 38
/
/
/
/
41
/
/
/
/
/
/
/
/
Internals number / type 39 Material 40 42 43 44 45 46
Cold, external
47 Insulation 48 Remarks: row 17) To be finally decided by tray manufacturer / contractor row 18) Only applicable if density > 1000 kg/m
a 0 . v e R
3
(62.43 lb/ft3)
row 16) To be finally decided by tray and demister manufacturer / contractor. rows 21) and 22) Stream out conditions are to be specified by detailed engineering contractor, if required. row 26) Base material can be CS cladded with SS316L. General Notes: - For tray design use information specified in document "General Notes for Column ". - Refer to "General Notes for Equipments "
s l x . s n o i t c e S r o t c a e R n m u l o C S D s s e c o r P i g r u L
Line revised under Rev. No.
Project Name Case-Name:
Normal Case
Project No.
Document No. Printed by / date / time:
Sheet / of 2 / 7 /
Revision 00 /
Process Process Data Sheet
Nozzle / d n a n o i t a n i m e s s i d , n o i t c u d o r p e r o t d e t i
n i d e z i r o h t u a y l s s e r p x e s s e l n u d e t i b i h o r p m y i l l t t c o i r n t s t u e b r g a s n t i d n e u t l c n n o i c , n t s o i i t d a n z i a l i t t u n e r e m h u t o c o r o d / s d i h n t a f n o , o i t n a i o t i t o u l b p i r x t e i s y d n r A o
01 Item Number
y r a t e i r p o r p l l a o t d e t i m i l t o n t u b g n i d u l c n i , s t h g i r l l A . s e g a
06-T-0101
02
. d e v r e s e r e r a , s t h g i r y t r e p o r p l a i r t s u d n i r e h t o r o / d m n a a d l s r e o d f e o l b m a y i t l i l i e t r a u , s t s r e n e d t n a e p f f o O t . i n g o r i u t a L l e r y b n i g s n t i t h i r i g w r
06
Unit Number
03
Unit Name
Rectisol
Description
Ammonia Scrubber I
04 Table of Nozzles
05 06
Item
No req
08
N1
1
3
Sour Water out to B.L.
09
N2
1
30
Raw Synthesis Gas in from 06-E-0102
10
N3
1
3
HP-Boiler Feed Water in from 06-E-0103
11
N4
1
30
Raw Synthesis Gas out to 06-E-0104/E-0105
12
V1
1
2
Vent (Blind)
13
D1
1
2
Drain
14
P1
1
2
Pressure Indicator
15
L1A/B
2
2
Level Gauge
16
L2A/B
2
2
Level Transmitter
17
L3A/B
2
2
Level Transmitter
18
L4A/B
2
2
Level Transmitter
19
M1 - M2
2
24
Manhole
07
NPS in
Rating
Facing
Designation
20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 Remarks: Rating and Facing according pipe-class
a 0 . v e R
s l x . e l z z o N S D s s e c o r P i g r u L
Line revised under Rev. No.
Project Name Case-Name:
Normal Case
Project No.
Document No. Printed by / date / time:
Sheet / of 3 / 7 /
Revision 00 /
Process Process Data Sheet
Sketch / d n a n o i t a n i m e s s i d , n o i t c u d o r p e r o t d e t i m i l t o n t u b g n i d u l c n i , n o i t a z i l i t u r e h t o r o / d n a n o i t a t i o l p x e y n A
n i d e z i r o h t u a y l s s e r p x e s s e l n u d e t i b i h o r p y l t c i r t s e r a s t n e t n o c s t i d n a t n e m u c o d s i h t f o , n o i t u b i r t s i d r o
y r a t e i r p . o r d p e l v l r a e o s t e d r e e r t i a m , i l s t t o h g n i r t u y b t r g e n p i o d r u p l l c a n i i r , t s s t u h d g i n i r r l l e A h . t o s e r g o a / d m n a a d l s r e o d f e o l b m a t y i l i l e i t r a u , s t s r e n e d t n a e p f f o O t . i n g o r i u t a L l e r y b n i g s n t i t h i r i g w r
01 Item Number 02
06
Unit Number
06-T-0101
03
Unit Name
Rectisol
Description
Ammonia Scrubber I
04
N4
05 06
P1
V1
07 08 09 10
T.L.
11 12
8"
13
Mesh Demister
14 " 6 5
15 16
4"
17 18
M2
N3
19
1
20
" 2 7 = 4 2 X 3
21 22 23 24 25 "
1) Distributor to be designed by internals Vendor / Contractor
2
2
26 8 2
4
27
. 28 L . T 29 . L 30 T
N2
1)
31 32 33 " 4 5 1
34 35
L1B,L2B, L3B, L4B
36
ID134"
37 38
" 8 1
39
M1
40 41 42 43
" 0 1
44
L1A ,L2A, L3A, L4A
45 46
T.L.
Vortex Breaker
47 48 49 50
N1
2)
51 52
D1
53 54 55
a 0 . v e R
s l x . h c t e k S S D s s e c o r P i g r u L
56
2)
57
Minimum required for piping
Heat tracing for winterizing
Line revised under Rev. No.
Project Name Case-Name:
Normal Case
Project No.
Document No. Printed by / date / time:
Sheet / of 4 / 7 /
Revision 00 /
Process Process Data Sheet
Tray / d n a n o i t a n i m e s s i d , n o i t c u d o r p e r o t d e t i
n i d e z i r o h t u a y l s s e r p x e s s e l n u d e t i b i h o r p m y i l l t t c o i r n t s t u e b r g a s n t i d n e u t l c n n o i c , n t s o i i t d a n z i a l i t t u n e r e m h u t o c o r o d / s d i h n t a f n o , o i t n a i o t i t o u l b p i r x t e i s y d n r A o
01 Item Number
y r a t e i r p o r p l l a o t d e t i m i l t o n t u b g n i d u l c n i , s t h g i r l l A . s e g a
06-T-0101
02
. d e v r e s e r e r a , s t h g i r y t r e p o r p l a i r t s u d n i r e h t o r o / d m n a a d l s r e o d f e o l b m a y i t l i l i e t r a u , s t s r e n e d t n a e p f f o O t . i n g o r i u t a L l e r y b n i g s n t i t h i r i g w r
06
Unit Number
03
Unit Name
Rectisol
Designation
Ammonia Scrubber I
04 05 Column section number Top
06 Column section designation
Bottom
07 08 Tray No.
1
from to
4
09 Operating data of decisive tray No. 10
Operating pressure
11
Medium
12 13 14 15 16
y a r t o t r u o p a V
psi [a]
Operating temperature t op Normal load Required load
min. max.
Molecular weight Density @ t op
17
Dynamic viscosity @ t
18
Compressibility factor Z = p·V / R·T
19 20 21 22
op
822.5
823.2
Shifted Raw Gas
Shifted Raw Gas
50
50
lb/h
1097599
1097687
%
50.00
105.00
50.00
110.00
lb/lbmol
21.34
21.34
lb/ft³
3.31
3.32
cP
0.02
0.02
0.97
0.97
Sour Water
Sour Water
54
50
°F lb/h min. max.
4 4
°F
Medium y Operating temperature a r t Normal load m o r f Required load d i Density @ t u op q i L Dynamic viscosity @ t op
1
1
%
29135 50.00
110.00
29223 50.00
110.00
lb/ft³
64.51
64.52
cP
1.19
1.25
dyn/cm
74.51
74.77
26 Allowable pressure drop per tray
psi
0.11
0.11
27 Allowable level in the downcomer
in
%
80
80
1
1
134
134
Bubble-cap
Bubble-cap
24
24
1
1
SS 316L
SS 316L
SS 316L
SS 316L
23 24 25
Surface tension
28 Allowable hold-up time in the downcomer
h lb/h
29 Allowable leakage rate per tray 30 Allowable flooding factor 31 Foaming factor (system factor) 32 Column inside
calculated
in
33 diameter
selected
in
34 Type of tray in
35 Tray spacing 36 Number of passes 37 38 39
l Tray a i r Valve e t a Bubble M
or tunnel caps
40 41 Remarks: row 8, 9) Count from
top
row 32, 35) To be stated b y tray manufacturer General Notes -Internals to be installed into t he column/vessel through manhole. -Maximum recommended downcomer inlet velocity: 0.39 ft/s -Maximum recommended downcomer clear liquid backup: 40%, I.e. 0.4 (Tray Spacing +Outlet weir height) -For tray design use information specified in docum ent "General Notes for Columns" -Trays to be seal welded to support ring and between segments -Manway to be carefully sealed -Picked fenced weir to be applied for p roper liquid distribution
a 0 . v e R
s l x . y a r T S D s s e c o r P i g r u L
Line revised under Rev. No.
Project Name Case-Name:
Normal Case
Project No.
Document No. Printed by / date / time:
Sheet / of 5 / 7 /
Revision 00 /
Process Process Data Sheet
Demister / d n a n o i t a n i m e s s i d , n o i t c u d o r p e r o t d e t i
n i d e z i r o h t u a y l s s e r p x e s s e l n u d e t i b i h o r p m y i l l t t c o i r n t s t u e b r g a s n t i d n e u t l c n n o i c , n t s o i i t d a n z i a l i t t u n e r e m h u t o c o r o d / s d i h n t a f n o , o i t n a i o t i t o u l b p i r x t e i s y d n r A o
y r a t e i r p o r p l l a o t d e t i m i l t o n t u b g n i d u l c n i , s t h g i r l l A . s e g a
01 Item Number
06-T-0101
02
. d e v r e s e r e r a , s t h g i r y t r e p o r p l a i r t s u d n i r e h t o r o / d m n a a d l s r e o d f e o l b m a y i t l i l i e t r a u , s t s r e n e d t n a e p f f o O t . i n g o r i u t a L l e r y b n i g s n t i t h i r i g w r
06
Unit Number
03
Unit Name
Rectisol
Designation
Ammonia Scrubber I
04 Top
05 Column section 06
Wire Mesh
07 Type of mist eliminator 08 09 10 11
14
Sour Water
Liquid
1096780
lb/h
Gas flow rate
MMSCFD
467.97
%
50.00
Gas
%
105.00
Liquid
%
110.00
12 Required turndown 13
Shifted Raw Gas
Gas
Fluids handled
Required overload
lb/h
15 Liquid at inlet (max) 17 Operating pressure p
54
°F
16 Operating temperature t op
psi[g]
op
821.8
Gas
lb/ft³
3.28
Liquid
lb/ft³
64.41
Gas
cP
0.02
Liquid
cP
1.19
22 Residual liquid
%
0.001
23 Degree of separation
%
99.99
µm
10
psi
0.2
18 19 20 21
24
Density @ t op , p op Viscosity @ t
op ,
p op
of droplets greater than
25 Allowable pressure drop 26 Free volume of wire mesh 27 Wire surface area
% ft²/ft³
28 Wire thickness (max.)
in
29 Wire thickness (min.)
in SS 316L
30 Material 31 Nozzle size (nominal pipe size)
in
30
32 Length x width, A x C
in
x
x
x
33 Height B / distance D
in
/
/
/
/
/
34 Arrangement A/B and angle 35 Remarks:
°
A
/
0
row 26-29) By manufacturer 1) By Manufacturer Surface Tension of liquid :74.50 dyne/cm 2) I nternals to be installed into the vessel throu gh manhole
Sketch
a 0 . v e R
s l x . r e t s i m e D S D s s e c o r P i g r u L
Line revised under Rev. No.
Project Name Case-Name:
Normal Case
Project No.
Document No. Printed by / date / time:
Sheet / of 6 / 7 /
Revision 00 /
Process Process Data Sheet
Nozzle Stream Table 01 Item Number / d n a n o i t a n i m e s s i d , n o i t c u d o r p e r o t d e t i m i l t o n t u b g n i d u l c n i , n o i t a z i l i t u r e h t o r o / d n a n o i t a t i o l p x e y n A
n i d e z i r o h t u a y l s s e r p x e
y r a t e i r p o r p l l a o t d e t i m i l t o n t u b g n i d u l c n i , s t h g i r l l A . s e g a m a d r o f e l b a i l
s s e l n u d e t i b i h o r p y l t c i r t s e r a s t n e t n o c s t i d n a t n e e r m a u s r c o e d d n s f e i f h t f O . o i , g n r o u i t L u y b b i r t g s i n i d t i r r o w
02 03 . d e v r e s e r e r a , s t h g i r y t r e p o r p l a i r t s u d n i r e h t o r o / d n a s l e d o m y t i l i t u , s t n e t a p o t n o i t a l e r n i s t h g i r
06
Unit Number
06-T-0101
Unit Name
Rectisol
Designation
Ammonia Scrubber I
04 Normal Case
05 Case N1
06 Nozzle-ID
N2
Sour Water out to B.L.
07 Nozzle designation
N3
N4
Raw Synthesis Gas in from HP-Boiler Feed Water in 06-E-0102
08
Raw Synthesis Gas out to
from 06-E-0103
06-E-0104/E-0105
102
09 Stream no. 10 Internal stream no.
123
102
122
103
Sour Water
Raw Syn Gas I
HP Boiler Feed Water
Raw Syn Gas I
from 06-T-0101
to 06-T-0101
to 06-T-0101
(scrubbed)
Liquid
Mixed
Liquid
Vapour
11 Stream designation 12
103
1 3 Pha se 14 Total flow
lbmol/h
1693.2
51553.8
1569.7
51415.4
15 Total flow
lb/h
31054
1099809
28278
1096750
16 ft³/h
17 Vol. flow 18 Norm. vol. flow
lbmol/h
Liquid 481.30
Vapour -
Liquid 32.89
Vapour 51436.9
Liquid 453.59
Vapour
Liquid
Vapour
-
51415.4
-
19 Mass flow
lb/h
31054
2122
1097688
28278
20 Mole flow
lbmol/h
1693.2
115.8
51438.0
1569.7
51415.4
21 Molweight
lb/lbmol
18.34
18.33
21.34
18.02
21.33
lb/ft³
64.52
64.49
3.32
62.34
3.28
Btu/(lb °F)
0.99
0.99
0.38
1.00
0.38
cP
1.25
1.24
0.02
0.67
0.02
25 Ther. conductivity (Btu/h)/(ft °F) fraction 26 Mole fraction fraction 27 Mass fraction
0.23
0.23
0.03
0.36
0.03
1.00
0.00
1.00
1.00
1.00
1.00
1.00
22 Eff. density 23 Spec. heat cap. 24 Viscosity
1.00
°F
28 Temperature
psi [a]
29 Pressure
0.00
1096750
1.00
50
50
104
54
823.2
823.2
829.0
821.8
30 31 Nozzle-ID 32 Nozzle designation 33 34 Stream no. 35 Internal stream no. 36 Stream designation 37 3 8 Pha se 39 Total flow
lbmol/h
40 Total flow
lb/h
41
Liquid ft³/h
42 Vol. flow 43 Norm. vol. flow
lbmol/h
44 Mass flow
lb/h
45 Mole flow
lbmol/h
46 Molweight
lb/lbmol
Vapour
Liquid
-
Vapour
Liquid
-
Vapour
Liquid
Vapour
-
-
lb/ft³
47 Eff. density 48 Spec. heat cap.
Btu/(lb °F) cP
49 Viscosity
50 Ther. conductivity (Btu/h)/(ft °F) fraction 51 Mole fraction 52 Mass fraction s l x . e l b a T m a e r t S e l z z o N S D s s e c o r P i g r u L
fraction °F
53 Temperature
psi[g]
54 Pressure 55 Remarks:
a 0 . v e R
Line revised under Rev. No.
Project Name Case-Name:
Normal Case
Project No.
Document No. Printed by / date / time:
Sheet / of 7 / 7 /
Revision 00 /
