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Université de Marne la Vallée Maîtrise de Physique et Applicat Applications ions Option Matériaux
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Les matériaux métalliques Introduction : qu’est-ce qu’un métal ? I – Quelq Quelques ues rappels rappels sur les métaux - Pro Propri priété étéss des métau métauxx - St Stru ruct ctur ures es - él élec ectro troni niqu ques es Master your semester with Scribd Read Free Foron 30this Days Sign up to vote title - cri cristal stallog lograp raphiq hiques ues & The New York Times Not useful - Contrai Contraintes ntes et déform déformations ations Useful Cancel anytime. Special offer for students: $4.99/month. II –Only Elabor Ela borati ation on des des métaux métaux eu d’h d’his isto toir iree (« ch chéo éo étal étallu lu ie »)
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Les matériaux métalliques Introduction : qu’est-ce qu’un métal ? I – Quelq Quelques ues rappels rappels sur les métaux - Pro Propri priété étéss des métau métauxx - St Stru ruct ctur ures es - él élec ectro troni niqu ques es Master your semester with Scribd Read Free Foron 30this Days Sign up to vote title - cri cristal stallog lograp raphiq hiques ues & The New York Times Not useful - Contrai Contraintes ntes et déform déformations ations Useful Cancel anytime. Special offer for students: $4.99/month. II –Only Elabor Ela borati ation on des des métaux métaux eu d’h d’his isto toir iree (« ch chéo éo étal étallu lu ie »)
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BIBLIOGRAPHIE
Physique du solide !- C. KITTEL - Physique de l’état solide - Dunod- 5ème édition - 1983 - M. BROUSSEAU - Physique du solide, Propriétés électroniques - Masson -1992 - J. CAZAUX - Initiation à la physique du solide , exercices commentés - Masson 199
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INTRODUCTION QU’EST-CE QU’UN METAL ? C’es t u n é lé m en t q u i p o s s èd e :
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u cNot tuuseful re é lec tr o n Useful s tr Cancel anytime.
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Les différentes classes de métaux : 1)
les métaux « nobles » (Au, Ag, Pt) p eu r é ac ti fs (no n -ox y d ab les ) s e r en c o n tr en t àl’ é tat «n atif »(pu r) d an s la n atu re
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(en p ar ti c u lier av ec les g az h alo g èn es ) remp lissage niveaux s You'redes Reading a Preview
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Les métaux et Mendeleïev non-métaux
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p
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Origine des gisements métalliques terrestres en 5 é tap es …
1ère étape : le « big-bang » : -13,8 m illiar ds
d’ an né es (env iro n… )
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étoile de grande taille (M>1,5Ms) étoiles massives
H
(>1,5 M)
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es ) 3ème étape : formation de la terre par accrétion (100 m il li o n s d ’an n é
poussières (Si, O, Fe…)
ac c ré tio n
ac cré tio n
ag g lo m é ra ti o n
astéroïdes
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Les métaux lourds se rassemblent au centre, les éléments légers vers la sur
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es ) 4ème étape : bombardement météoritique (<1 m il li ar d d ’an n é
Le bombardement par des météorites va enrichir la surface de la terre par des métaux lourds
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es ) 5ème étape : formation de gisements métallifères (d es m il li o n s d’ an n é
dissolution (eau)
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transport
!
précipitation
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I - CARACTERISTIQUES
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Structure électronique structure de bande métallique :
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le n iv eau d e Ferm i es t àl’i n té rieu r d e la b and e d e co n d u ct io n
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Pas t ou t àfait ex act… car le p ot enti el est m od ulépar les io ns de plus il peut y avoir chevauc hement de bandes
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métaux de transition remp lissage de la so us c ouc he d et chevauchem ent avec la sou s co uche
s et p ne forment qu’une seule bande très large (>2 que la bande d est plus étroite (5eV)
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Conséquences :
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le ferromagnétisme
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La couleur de certains métaux
la plupart des métaux sont brillant (réflexion totale de la lumière) d’autres (Cu,semester Au) présentewith une Scribd Master your Read Free Foron 30this Days Sign up to vote title couleur résultant d’une absorption & The New York Times Useful Not useful de certaines longueurs d’onde) Cancel anytime. Special Cette offer for absorption students: Only $4.99/month. est due aux électrons 3d proches du niveau You're Reading a Preview
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Notions de cristallographie
cristal : structure périodique d’atomes ou de molécules à 3 dimensions
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structure B2 (CsCl, FeAl, NiAl… réseau cubique
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Structures cristallographiques
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[uvw] direction cristallogr famille de direction
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exemple d’indice
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Cas de la structure hexagonale 4 indices de Miller : h, k, i et l avec i=-(h+k)
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Structure hexagonale : définition des différentes familles de plans cristallographiques et des systèmes de glissement
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La plupart des métaux cristallisent dans un réseau cubique
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Le taux de remplissage de l’espace de la structure bcc est de 68% Celui des structures fcc et hc est de 74% (taux maximum) : ce sont des structures com pactes Elles n e dif fé ren t q u e par l a su cc ess io n des plans cristallogr aphiques
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Quelques rappels sur les défauts cristallographiques défaut : - échelle macroscopique : défaut d’homogénéité - échelle atomique : dû à l’absence ou au déplacements d’atomes
ordre 0 (0D) : défaut ponctuel (lacune et interstitiel) ordre 1 (1D) : défaut linéaire (dislocations) Master your semester with Scribd ordre 2 (2D) : surface libre, défaut plan… Read Free Foron 30this Days Sign up to vote title ordre 3 (3D) : ségrégations, cavités, fissures, inclusions
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atome interstitiel de petit
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défauts ponctuels : diffusion atomique les différents mécanismes
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Les défauts linéaires : les dislocations
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cris tal parfait
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Mouvement des dislocations mouvement conservatif (sans déplacement de matière) : glissement mouvement non-conservatif (avec déplacement de matière) : montée 1) Glissement (glide)
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dans une direction particulière.
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2) Le glissement dévié (cross-slip)
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La ligne de dislocation xyzw pos des composantes coin pures (y e des vis pures (x et z). La dislocation vis n’ayant pas de glissement associé défini, elle pe changer de direction lorsqu’elle (c et un autre plan deon30 glissement Read Free For Days Sign up to vote this title C’estleUseful glissement dévié. Not useful
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Origine du déplacement
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une force F appliquée au cristal entraîne l’apparition d’une contrainte de cisaillement « résolue » au niveau du plan de glissement (slip plan):
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Interactions entre dislocations
lorsque 2 dislocations de sign ayan t m êm e plan d e glis sem en peuvent s’annihiler
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formation de crans par intersection de lignes de dislocations
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intersections de 2 dislocations : formation de jonctions
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Multiplication (sources) de dislocation autour de précipités sous l’action d’une contrainte
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Observations de dislocations par microscopie électronique en transmission
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Fe bcc : dislocation
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Pourquoi les dislocations ? rupture des liaisons atomiques :
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σ = Eε
Il y aura rupture lorsque ε ≥ 0,25r
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déformation plastique et dislocations dislocation : moyen le plus simple (en terme énergétique) de déformer le métal par déplacement d’une quantité réduite d’atomes…
s im ilai r e à: -le déplacement d’une cheni
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Une contrainte extérieure appliquée à un cristal : - écartement des atomes (il apparaît une force de rappel) - déformation élastique (réversible) tant que r<1,25r 0 - si la contrainte est supérieure à la force de cohésion, rupture locale d
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Durcissement par interactions défauts dislocation
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Les défauts plans - défaut d’empilement cfc : succession de plans ABCABCABC… représentation : """"""""""""" perturbation dans la succession : ABCABABCABC…
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Microstructure des métaux monophasée ou multiphasée
métal pur, alliage
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différ struc ordo
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monophasée ou multiphasée
un alliage peut c ontenir n d es in c lu sio n s et d es
alliage multiphasé exem pl e : aciers aus té no ferri tiq ues ou «duplex »
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Structure microscopique des métaux
Structure en « grains » (petits domaines cristallins de structure identique mais d’orientations différentes)
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Les propriétés du matériau dépendent de la forme et de la taille des grain
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la l im it e é las ti q u e d ’u n ac ier p eu t être d o u b lé e s i la t ail le d es g ra in s es t d iv is é e p ar 10… dans le cas d es nano str uc tur es (grain s de l’or dre de qu elques n anom on peu t o bs erv er uwith ne s upScribd erpl astic ité … your semester
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peuvent modifier la forme et la taille des grains
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les joints de grains ...
θ
première hypothèse (abandonnée vers les années 30...) : existence d'un "ciments" pour tenir la cohésion des grains En fait, le joint (démontré au début des années 60) est une ligne immatérielle entre 2 grains de structure identique mais d'orientation différente
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- joints de forte désorientation (θ>15°)
On peut caractériser un tel joint par le réseau de co (CSL) c’est à dire le réseau formé par les atomes d qui se superposent (en les imaginant s’interpénétra
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En général le joint de grains est une zone très fortement désordonnée Sa densité peut ne représenter que 50% de celle du grain Sa forte densité en défauts ponctuels (lacunes) et linéaires (dislocations) favorise les phénomènes de diffusion (coefficients de diffusion supérieurs de plusieurs ordres de grandeurs à ceux en volume), de précipitation (précipitation hétérogène)with et de ségrégations. Master your semester Scribd Read Free Foron 30this Days Sign up to vote title
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intercristalline) peuvent fragiliser les joints de grain provoquer des ruptures intergranulaires. You're Reading a Preview
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La texture
Dans un échantillon polycristallin la distribution des orientations cristallines peut être a Dans ce cas les caractéristiques du matériau sont isotropes… Il arrive fréquemment qu’une anisotropie apparaisse : les caractéristiques mécaniques, physiques etc sont différentes selon la direction. cette anisotropie peut être due à plusieurs facteurs : - répartitions des contraintes internes Master your semester with Scribd - ségrégations chimiques des impuretés Read Free Foron 30this Days Sign up to vote title - forme des grains & The New York Times Useful Not useful Cancel anytime. plus généralement, orientation non aléatoire des grains $ texture Special offer for students: Only $4.99/month. You're Reading a Preview
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La texture peut avoir des conséquences sur le comportement mécanique et sur les propriétés liées aux joints de grains (diffusion, ségrégation, fluage…) certaines propriétés isotropes peuvent devenir anisotropes sous forte texture… La texture peut être mesurée (diffraction des rayons X, EBSD…) Elle est caractérisée par les figures de pôles : Master your semester with Scribd & The New York Times Special offer for students: Only $4.99/month.
normale
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trois p lans {
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Exemple d’analyse de texture par EBSD image EBSD
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Joints de phases
surface séparant deux phases (généralement un précipité ou une inclus et la matrice) Ce joint peut être :
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Comportement mécanique : quelques définitions
Courbe d
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